Module Details
Module Code: |
ZINS C2101 |
Module Title:
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Instrumentation
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Title:
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Instrumentation
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Module Level:: |
6 |
Module Coordinator: |
Paula Rankin
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Module Author:: |
John Cleary
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Module Description: |
The aim of this module is to provide the student with an introduction to the principles and operation of a range of analytical instrumentation and to develop practical laboratory skills in the use of such instrumentation.
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Learning Outcomes |
On successful completion of this module the learner will be able to: |
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Learning Outcome Description |
LO1 |
Describe the physical principles, components and operation of analytical and process control instrumentation. |
LO2 |
Identify sources of uncertainty in measurement in analytical instrumentation. |
LO3 |
Demonstrate the necessary skills to evaluate equipment for a particular use and to maintain and optimise the operation of this equipment. |
LO4 |
Identify hazards and evaluate risks in an analytical laboratory. |
LO5 |
Apply relevant computer software for data analysis and reporting. |
Dependencies |
Module Recommendations
This is prior learning (or a practical skill) that is recommended before enrolment in this module.
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No recommendations listed |
Co-requisite Modules
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No Co-requisite modules listed |
Additional Requisite Information
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No Co Requisites listed
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Indicative Content |
Measurement and metrology
Types of error, Identifying and analysing error and uncertainty, Accuracy and precision, Instrument specifications and performance, Reporting and interpretation of results.
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Measurement of Physical Properties
Physical principles and operation of polarimeter, viscometers (manual and rotational), refractometer, hydrometer, density bottle.
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Principles of optics and optical systems
Electromagnetic spectrum. Wavelength, frequency, energy of radiation. Absorbance, transmittance, Beer's law. Optical parameters - resolution, resolving power, dispersion.
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Spectrometers and Spectroscopy
Spectrophotometers and components (UV-visible and fluorescent spectroscopies, Infrared spectroscopy) Atomic spectroscopy (AAS, GF-AAS, ICP-AES). Light sources. Wavelength selection: filters, prisms, gratings, monochromators. Detectors (photomultipliers, photodiode, thermal). Characteristics of detectors (sensitivity, noise, response time, spectral range, stability), Comparison of single beam and dual beam systems. Errors in spectroscopy.
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Sensors and transducers
Physical principles and types of transducers for measurement of temperature, sound, pressure, flow, level. Transducer specifications - range, sensitivity, response time, linearity. Measurement of pH, O2, CO2. Introduction to Biosensors.
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Data acquisition and process control.
Introduction to automation in industrial processes. Signal conditioning. Single and multivariable control loops. Types of control: on/off, closed loop, proportional, integral and derivative (PID) control. Fluid dynamics and the design and operation of valves and pumps.
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Module Content & Assessment
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Assessment Breakdown | % |
Continuous Assessment | 20.00% |
Practical | 40.00% |
End of Module Formal Examination | 40.00% |
AssessmentsFull Time
End of Module Formal Examination |
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Reassessment Requirement |
Exam Board
It is at the discretion of the Examination Board as to what the qualifying criteria are.
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SETU Carlow Campus reserves the right to alter the nature and timings of assessment
Module Workload
Workload: Full Time |
Workload Type |
Workload Category |
Contact Type |
Workload Description |
Frequency |
Average Weekly Learner Workload |
Hours |
Lecture |
|
Contact |
Lecture |
12 Weeks per Stage |
4.00 |
48 |
Laboratory |
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Contact |
Practical class |
12 Weeks per Stage |
3.00 |
36 |
Estimated Learner Hours |
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Non Contact |
Independent learning |
15 Weeks per Stage |
11.07 |
166 |
Total Weekly Contact Hours |
7.00 |
Module Resources
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Recommended Book Resources |
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Douglas A. Skoog,F. James Holler,Stanley R. Crouch. (2017), Principles of Instrumental Analysis, 7th ed.. Nelson Education, p.992, [ISBN: 9781305577213].
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Robert M. Granger,Hank M. Yochum,Jill N. Granger,Karl D. Sienerth. (2018), Instrumental Analysis, Oxford University Press, USA, p.880, [ISBN: 9780190865337].
| Supplementary Book Resources |
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Alan S. Morris,Reza Langari. (2020), Measurement and Instrumentation, Academic Press, p.752, [ISBN: 9780128171417].
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Gary D. Christian,Purnendu K. Dasgupta,Kevin A. Schug. (2013), Analytical Chemistry, 7th ed.. John Wiley & Sons, p.848, [ISBN: 9780470887578].
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Brian R. Eggins. (2002), Chemical Sensors and Biosensors, John Wiley & Sons Incorporated, p.273, [ISBN: 0471899135].
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Curtis D. Johnson. Process Control Instrumentation Technology, 8th ed. [ISBN: 0131976699].
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Dr. Graham Currell. (2000), Analytical Instrumentation, Wiley, p.336, [ISBN: 0471999016].
| This module does not have any article/paper resources |
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Other Resources |
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LGC. LGC / National Measurement Institute,
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Sensors and Actuators B: Chemical, Elsevier,
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Spectroscopy Europe, Chichester, UK, IMP Open,
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World Health Organisation. (2008), Maintenance Manual for Laboratory
Equipment, Geneva, Switzerland, World Health Organisation,
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