Module Details

Module Code: ZINS C2101
Module Title: Instrumentation
Title: Instrumentation
Module Level:: 6
Credits:: 10
Module Coordinator: Paula Rankin
Module Author:: John Cleary
Domains:  
Module Description: The aim of this module is to provide the student with an introduction to the principles and operation of a range of analytical instrumentation and to develop practical laboratory skills in the use of such instrumentation.
 
Learning Outcomes
On successful completion of this module the learner will be able to:
# Learning Outcome Description
LO1 Describe the physical principles, components and operation of analytical and process control instrumentation.
LO2 Identify sources of uncertainty in measurement in analytical instrumentation.
LO3 Demonstrate the necessary skills to evaluate equipment for a particular use and to maintain and optimise the operation of this equipment.
LO4 Identify hazards and evaluate risks in an analytical laboratory.
LO5 Apply relevant computer software for data analysis and reporting.
Dependencies
Module Recommendations

This is prior learning (or a practical skill) that is recommended before enrolment in this module.
No recommendations listed
Co-requisite Modules
No Co-requisite modules listed
Additional Requisite Information
No Co Requisites listed
 
Indicative Content
Measurement and metrology
Types of error, Identifying and analysing error and uncertainty, Accuracy and precision, Instrument specifications and performance, Reporting and interpretation of results.
Measurement of Physical Properties
Physical principles and operation of polarimeter, viscometers (manual and rotational), refractometer, hydrometer, density bottle.
Principles of optics and optical systems
Electromagnetic spectrum. Wavelength, frequency, energy of radiation. Absorbance, transmittance, Beer's law. Optical parameters - resolution, resolving power, dispersion.
Spectrometers and Spectroscopy
Spectrophotometers and components (UV-visible and fluorescent spectroscopies, Infrared spectroscopy) Atomic spectroscopy (AAS, GF-AAS, ICP-AES). Light sources. Wavelength selection: filters, prisms, gratings, monochromators. Detectors (photomultipliers, photodiode, thermal). Characteristics of detectors (sensitivity, noise, response time, spectral range, stability), Comparison of single beam and dual beam systems. Errors in spectroscopy.
Sensors and transducers
Physical principles and types of transducers for measurement of temperature, sound, pressure, flow, level. Transducer specifications - range, sensitivity, response time, linearity. Measurement of pH, O2, CO2. Introduction to Biosensors.
Data acquisition and process control.
Introduction to automation in industrial processes. Signal conditioning. Single and multivariable control loops. Types of control: on/off, closed loop, proportional, integral and derivative (PID) control. Fluid dynamics and the design and operation of valves and pumps.
Module Content & Assessment
Assessment Breakdown%
Continuous Assessment20.00%
Practical40.00%
End of Module Formal Examination40.00%

Assessments

Full Time

Continuous Assessment
Assessment Type Examination % of Total Mark 20
Timing Week 5 Learning Outcomes 1,2
Non-marked No
Assessment Description
1 hour exam
No Project
Practical
Assessment Type Practical/Skills Evaluation % of Total Mark 40
Timing Every Week Learning Outcomes 3,4,5
Non-marked No
Assessment Description
Practical log book
End of Module Formal Examination
Assessment Type Formal Exam % of Total Mark 40
Timing End-of-Semester Learning Outcomes 1,2
Non-marked No
Assessment Description
3 hour exam
Reassessment Requirement
Exam Board
It is at the discretion of the Examination Board as to what the qualifying criteria are.

SETU Carlow Campus reserves the right to alter the nature and timings of assessment

 

Module Workload

Workload: Full Time
Workload Type Workload Category Contact Type Workload Description Frequency Average Weekly Learner Workload Hours
Lecture Contact Lecture 12 Weeks per Stage 4.00 48
Laboratory Contact Practical class 12 Weeks per Stage 3.00 36
Estimated Learner Hours Non Contact Independent learning 15 Weeks per Stage 11.07 166
Total Weekly Contact Hours 7.00
 
Module Resources
Recommended Book Resources
  • Douglas A. Skoog,F. James Holler,Stanley R. Crouch. (2017), Principles of Instrumental Analysis, 7th ed.. Nelson Education, p.992, [ISBN: 9781305577213].
  • Robert M. Granger,Hank M. Yochum,Jill N. Granger,Karl D. Sienerth. (2018), Instrumental Analysis, Oxford University Press, USA, p.880, [ISBN: 9780190865337].
Supplementary Book Resources
  • Alan S. Morris,Reza Langari. (2020), Measurement and Instrumentation, Academic Press, p.752, [ISBN: 9780128171417].
  • Gary D. Christian,Purnendu K. Dasgupta,Kevin A. Schug. (2013), Analytical Chemistry, 7th ed.. John Wiley & Sons, p.848, [ISBN: 9780470887578].
  • Brian R. Eggins. (2002), Chemical Sensors and Biosensors, John Wiley & Sons Incorporated, p.273, [ISBN: 0471899135].
  • Curtis D. Johnson. Process Control Instrumentation Technology, 8th ed. [ISBN: 0131976699].
  • Dr. Graham Currell. (2000), Analytical Instrumentation, Wiley, p.336, [ISBN: 0471999016].
This module does not have any article/paper resources
Other Resources
Discussion Note: